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Appropriate Preparation Techniques. b Compounds CAS No a 3510 352 3541 355 3540/ 3580 0 0 3,3'-Dimethylbenzidine 119-93-7 X ND ND ND X α,α-Dimethylphenethylamine 122-09-8 ND ND ND ND X
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d) Rinse the eluate vials with 2 x 5 mL of DCM, transfer the rinses to the Na 2 SO 4 bed. Tip 5: If Na 2 SO 4 appears greenish, rinse with more solvent until it turns white. 8. Concentration a) Concentrate the eluates to 0.7-0.9 mL under a gentle stream of N 2 at 40 ºC. b) Add internal standards, transfer the extract to a 2-mL auto-sampler
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